Structures by: Sakamoto M.
Total: 168
C18H13NO3
C18H13NO3
Organic letters (2015) 17, 23 5846-5849
a=9.2686(15)Å b=16.156(3)Å c=9.4109(16)Å
α=90° β=95.246(2)° γ=90°
C25H33NO2
C25H33NO2
Photochemical & photobiological sciences : Official journal of the European Photochemistry Association and the European Society for Photobiology (2011) 10, 9 1387-1389
a=7.525(9)Å b=24.63(3)Å c=11.729(15)Å
α=90.00° β=98.548(18)° γ=90.00°
C13H10INO3
C13H10INO3
Organic letters (2013) 15, 24 6182-6185
a=20.2766(10)Å b=11.0112(6)Å c=13.5295(6)Å
α=90.00° β=123.314(2)° γ=90.00°
C19H22N2O2
C19H22N2O2
Organic letters (2011) 13, 23 6168-6171
a=16.127(2)Å b=9.1351(14)Å c=12.0699(17)Å
α=90.00° β=102.693(2)° γ=90.00°
C18H20N2O2
C18H20N2O2
Organic letters (2011) 13, 23 6168-6171
a=7.8221(5)Å b=14.5983(8)Å c=27.4837(16)Å
α=90.00° β=90.00° γ=90.00°
C20H24N2O2
C20H24N2O2
Organic letters (2011) 13, 23 6168-6171
a=8.8113(15)Å b=7.6399(13)Å c=13.258(2)Å
α=90.00° β=93.732(2)° γ=90.00°
3c
C20H26N2O2
Organic letters (2011) 13, 23 6168-6171
a=15.726(5)Å b=9.432(3)Å c=12.590(4)Å
α=90.00° β=103.660(4)° γ=90.00°
C12H10O4
C12H10O4
Organic letters (2010) 12, 20 4435-4437
a=4.6951(8)Å b=9.7328(16)Å c=22.307(4)Å
α=90.00° β=94.848(2)° γ=90.00°
C13H12O4
C13H12O4
Organic letters (2010) 12, 20 4435-4437
a=8.0748(7)Å b=9.2016(8)Å c=15.5271(13)Å
α=90.00° β=100.0840(10)° γ=90.00°
C22H16O8
C22H16O8
Organic letters (2010) 12, 20 4435-4437
a=9.1280(11)Å b=10.3355(12)Å c=10.6415(13)Å
α=76.6100(10)° β=68.8140(10)° γ=82.9290(10)°
C24H20O8
C24H20O8
Organic letters (2010) 12, 20 4435-4437
a=11.4827(9)Å b=11.0568(9)Å c=16.4519(13)Å
α=90.00° β=106.9240(10)° γ=90.00°
C26H24O8
C26H24O8
Organic letters (2010) 12, 20 4435-4437
a=6.5748(7)Å b=8.8652(10)Å c=10.7627(12)Å
α=69.1630(10)° β=82.4060(10)° γ=82.3500(10)°
C20H24N2O2
C20H24N2O2
Organic letters (2012) 14, 10 2638-2641
a=9.1324(11)Å b=12.9705(15)Å c=15.2515(18)Å
α=90.00° β=102.850(2)° γ=90.00°
C24H33N3O2
C24H33N3O2
Organic letters (2012) 14, 10 2638-2641
a=10.1320(12)Å b=15.1023(17)Å c=28.170(3)Å
α=90.00° β=90.00° γ=90.00°
C24H33N3O2
C24H33N3O2
Organic letters (2012) 14, 10 2638-2641
a=7.1143(18)Å b=16.557(4)Å c=18.936(5)Å
α=90.00° β=96.930(3)° γ=90.00°
C24H36N2O3
C24H36N2O3
Organic letters (2012) 14, 10 2638-2641
a=32.779(8)Å b=8.926(2)Å c=15.402(4)Å
α=90.00° β=94.480(3)° γ=90.00°
2i
C19H20N2OS
Organic & biomolecular chemistry (2018) 16, 42 7910-7919
a=13.0104(7)Å b=5.4301(3)Å c=24.2997(15)Å
α=90° β=101.772(4)° γ=90°
3j
C23H20N2OS
Organic & biomolecular chemistry (2018) 16, 42 7910-7919
a=8.887(2)Å b=9.348(2)Å c=12.182(3)Å
α=80.025(3)° β=72.125(3)° γ=88.273(3)°
3i
C19H20N2OS
Organic & biomolecular chemistry (2018) 16, 42 7910-7919
a=12.4130(15)Å b=17.816(2)Å c=7.9085(10)Å
α=90° β=106.841(2)° γ=90°
5c
C16H22N2O2S
Organic & biomolecular chemistry (2018) 16, 42 7910-7919
a=8.7745(14)Å b=9.4352(16)Å c=20.409(3)Å
α=93.504(2)° β=97.479(2)° γ=90.918(2)°
C38H40NP
C38H40NP
Organic & biomolecular chemistry (2019) 17, 6 1455-1465
a=9.3710(2)Å b=13.7203(3)Å c=11.5632(3)Å
α=90° β=93.1780(10)° γ=90°
C42H41Cl3NP
C42H41Cl3NP
Organic & biomolecular chemistry (2019) 17, 6 1455-1465
a=10.14120(10)Å b=17.5089(2)Å c=19.7319(3)Å
α=90° β=90° γ=90°
C41H42NP
C41H42NP
Organic & biomolecular chemistry (2016) 14, 31 7509-7519
a=10.5997(3)Å b=14.5202(4)Å c=21.0270(6)Å
α=90° β=90° γ=90°
C22H25N3O4
C22H25N3O4
Organic & Biomolecular Chemistry (2008) 6, 5 848-850
a=11.32160(10)Å b=13.26990(10)Å c=13.7391(2)Å
α=90.00° β=90.00° γ=90.00°
C22H25N3O4
C22H25N3O4
Organic & Biomolecular Chemistry (2008) 6, 5 848-850
a=8.0817(10)Å b=14.5195(18)Å c=17.141(2)Å
α=90.00° β=90.00° γ=90.00°
C19H18ClNO4
C19H18ClNO4
Organic & biomolecular chemistry (2014) 12, 39 7686-7689
a=6.6270(3)Å b=7.9739(3)Å c=32.9949(14)Å
α=90° β=90° γ=90°
(R)-N-(1-t-Butylethyl)-2-chromonecarboxamide
C16H19NO3
Organic & biomolecular chemistry (2014) 12, 47 9644-9649
a=5.9167(9)Å b=10.9747(17)Å c=12.2265(18)Å
α=64.4240(19)° β=82.5940(19)° γ=89.9950(19)°
(R)-N-(1-Phenylethyl)-2-chromonecarboxamide
C18H15NO3
Organic & biomolecular chemistry (2014) 12, 47 9644-9649
a=13.4156(6)Å b=13.4156(6)Å c=28.8130(14)Å
α=90° β=90° γ=120°
Anti-HH Photodimer of (R)-N-(1-phenylethyl)-2-chromonecarboxamide
C36H30N2O6
Organic & biomolecular chemistry (2014) 12, 47 9644-9649
a=12.2096(9)Å b=13.7443(10)Å c=18.0044(14)Å
α=90.00° β=90.00° γ=90.00°
Anti-HH photodimer of (R)-N-(1-phenylethyl)-2-chromonecarboxamide
C36H30N2O6
Organic & biomolecular chemistry (2014) 12, 47 9644-9649
a=9.7337(10)Å b=13.9495(14)Å c=22.104(2)Å
α=90.00° β=90.00° γ=90.00°
Anti-HH photodimer of (S)-N-(1-methoxycarbonylethyl)-2-chromonecarboxamide
C28H26N2O10
Organic & biomolecular chemistry (2014) 12, 47 9644-9649
a=8.021(3)Å b=15.273(5)Å c=21.484(7)Å
α=90.00° β=90.00° γ=90.00°
Anti-HH photodimer of (S)-N-(1-methoxycarbonylethyl)-2-chromonecarboxamide
C39H41N3O12
Organic & biomolecular chemistry (2014) 12, 47 9644-9649
a=12.380(5)Å b=12.380(5)Å c=42.393(17)Å
α=90.00° β=90.00° γ=120.00°
C25H20ClNO4
C25H20ClNO4
Organic & biomolecular chemistry (2017) 15, 2 320-323
a=6.5505(3)Å b=8.7111(4)Å c=9.9103(5)Å
α=82.5366(18)° β=73.6985(14)° γ=76.9181(18)°
C38H40NP
C38H40NP
Organic & biomolecular chemistry (2016) 14, 31 7509-7519
a=10.51380(10)Å b=14.5405(2)Å c=19.6851(3)Å
α=90° β=90° γ=90°
C41H40NP
C41H40NP
Organic & biomolecular chemistry (2016) 14, 31 7509-7519
a=10.61960(10)Å b=22.1572(2)Å c=26.8016(3)Å
α=90° β=90° γ=90°
C16H14N2O
C16H14N2O
Organic & biomolecular chemistry (2010) 8, 23 5418-5422
a=7.3179(6)Å b=15.6561(13)Å c=11.4483(10)Å
α=90.00° β=103.4610(10)° γ=90.00°
C16H14N2S
C16H14N2S
Organic & biomolecular chemistry (2010) 8, 23 5418-5422
a=7.6223(3)Å b=7.6223(3)Å c=23.186(2)Å
α=90.00° β=90.00° γ=90.00°
C16H14N2O2
C16H14N2O2
Chemical Communications (2000) 13 1201
a=17.024(6)Å b=29.192(7)Å c=11.183(4)Å
α=90° β=90° γ=90°
C16H14N2O2
C16H14N2O2
Chemical Communications (2000) 13 1201
a=9.903(2)Å b=10.132(2)Å c=7.430(1)Å
α=91.75(1)° β=105.73(2)° γ=108.74(1)°
C16H17NO2
C16H17NO2
Chemical Communications (Cambridge, United Kingdom) (2007) 34 3586-3588
a=7.6281(15)Å b=11.856(2)Å c=14.408(3)Å
α=90.00° β=90.00° γ=90.00°
7008963
Journal of the Chemical Society, Dalton Transactions (2000) 3 259
a=17.354(3)Å b=14.050(3)Å c=17.780(3)Å
α=90° β=105.45(1)° γ=90°
7008964
Journal of the Chemical Society, Dalton Transactions (2000) 3 259
a=17.312(2)Å b=14.030(1)Å c=17.765(2)Å
α=90° β=106.093(7)° γ=90°
C21H16CuN2O2
C21H16CuN2O2
Journal of the Chemical Society, Dalton Transactions (2000) 3 259
a=11.516(2)Å b=8.972(2)Å c=16.562(2)Å
α=90° β=98.86(1)° γ=90°
2h
C19H20N2OS
Organic & biomolecular chemistry (2018) 16, 42 7910-7919
a=12.8458(5)Å b=5.3427(2)Å c=24.6144(10)Å
α=90° β=101.767(3)° γ=90°
4g
C18H18N2OS
Organic & biomolecular chemistry (2018) 16, 42 7910-7919
a=34.665(4)Å b=6.9265(9)Å c=14.4146(18)Å
α=90° β=113.1370(10)° γ=90°
2j
C23H20N2OS
Organic & biomolecular chemistry (2018) 16, 42 7910-7919
a=13.613(2)Å b=5.3251(9)Å c=26.026(4)Å
α=90° β=95.958(3)° γ=90°
Anti-HH photodimer of (R)-N-(1-t-butylethyl)-2-chromonecarboxamide
C32H38N2O6
Organic & biomolecular chemistry (2014) 12, 47 9644-9649
a=7.704(18)Å b=14.23(3)Å c=26.50(6)Å
α=90° β=90° γ=90°
C50H64BCl3N2O9Zn2
C50H64BCl3N2O9Zn2
Journal of the Chemical Society, Dalton Transactions (1999) 6 997
a=14.626(1)Å b=16.343(2)Å c=13.398(1)Å
α=99.200(2)° β=114.834(1)° γ=69.368(4)°
C42H64AuF6N2PS2
C42H64AuF6N2PS2
Dalton transactions (Cambridge, England : 2003) (2013) 42, 45 15995-16005
a=14.1525(19)Å b=17.312(2)Å c=28.758(4)Å
α=79.331(4)° β=86.571(4)° γ=81.644(5)°
N-(2,5-dimethylphenyl)monothiosuccinimide
C12H13NOS
Chemical communications (Cambridge, England) (2003)
a=10.847(3)Å b=6.580(2)Å c=8.505(2)Å
α=90.00° β=105.76(2)° γ=90.00°
5-(2,5-Dimethyl-phenyl)-3,3-diphenyl-1-thia-5-aza- spiro(3.4)octan-6-one
C29H32NOS
Chemical communications (Cambridge, England) (2003)
a=9.851(3)Å b=9.336(2)Å c=27.569(9)Å
α=90.00° β=107.60(9)° γ=90.00°
C18H19NO2
C18H19NO2
Chemical communications (Cambridge, England) (2004) 8 1002-1003
a=10.937(5)Å b=13.987(5)Å c=9.896(4)Å
α=90.00° β=90.00° γ=90.00°
C23H21NO2
C23H21NO2
Chemical communications (Cambridge, England) (2004) 8 1002-1003
a=14.384(4)Å b=16.234(5)Å c=8.049(4)Å
α=90.00° β=90.00° γ=90.00°
C28H23NO2
C28H23NO2
Chemical communications (Cambridge, England) (2004) 8 1002-1003
a=19.753(5)Å b=22.214(7)Å c=9.936(3)Å
α=90.00° β=90.00° γ=90.00°
C16H13NO2
C16H13NO2
Chem.Commun. (2013) 49, 4776
a=13.1134(11)Å b=13.6354(11)Å c=7.2439(6)Å
α=90.00° β=90.00° γ=90.00°
C22H17NO2
C22H17NO2
Chem.Commun. (2013) 49, 4776
a=17.1516(3)Å b=11.5890(2)Å c=8.4053(2)Å
α=90.00° β=90.00° γ=90.00°
C24H21NO2
C24H21NO2
Chem.Commun. (2013) 49, 4776
a=11.729(4)Å b=8.588(3)Å c=37.580(13)Å
α=90.00° β=90.00° γ=90.00°
C23H19NO2
C23H19NO2
Chem.Commun. (2013) 49, 4776
a=8.8218(6)Å b=17.4333(12)Å c=11.8783(9)Å
α=90.00° β=100.3140(10)° γ=90.00°
C60H69Cl2NO2P4Rh2
C60H69Cl2NO2P4Rh2
Chem.Commun. (2013) 49, 5250
a=13.687(5)Å b=14.485(6)Å c=29.226(11)Å
α=90.0000° β=91.683(6)° γ=90.0000°
C53H55Cl8NP4Rh2
C53H55Cl8NP4Rh2
Chem.Commun. (2013) 49, 5250
a=13.404(7)Å b=14.372(8)Å c=30.132(12)Å
α=90.0000° β=95.9511(12)° γ=90.0000°
C60H64.50Cl2N5.50O2P4Rh2
C60H64.50Cl2N5.50O2P4Rh2
Chem.Commun. (2013) 49, 5250
a=12.604(6)Å b=12.861(5)Å c=20.226(9)Å
α=73.940(7)° β=80.980(6)° γ=74.474(7)°
C47H51Cl4NO2P4Rh2
C47H51Cl4NO2P4Rh2
Chem.Commun. (2013) 49, 5250
a=29.706(15)Å b=14.423(7)Å c=11.405(6)Å
α=90.0000° β=90.0000° γ=90.0000°
C16H17NO2
C16H17NO2
Chemical Communications (Cambridge, United Kingdom) (2007) 34 3586-3588
a=7.6281(15)Å b=11.856(2)Å c=14.408(3)Å
α=90.00° β=90.00° γ=90.00°
(S,aR)-1a
C18H19NO4
Chemical communications (Cambridge, England) (2007) 16 1632-1634
a=11.0267(17)Å b=6.9804(11)Å c=11.2114(17)Å
α=90.00° β=116.392(2)° γ=90.00°
(S,aR)-1b
C19H21NO4
Chemical communications (Cambridge, England) (2007) 16 1632-1634
a=7.6654(5)Å b=12.7990(8)Å c=9.0881(6)Å
α=90.00° β=99.4860(10)° γ=90.00°
(S)-2b
C34H30N2O4
Chemical communications (Cambridge, England) (2007) 16 1632-1634
a=10.1974(5)Å b=12.5011(6)Å c=21.8192(10)Å
α=90.00° β=90.00° γ=90.00°
C22H19NOS
C22H19NOS
Chemical Communications (2006) 44
a=6.126(3)Å b=9.050(4)Å c=32.991(11)Å
α=90.00° β=90.00° γ=90.00°
C20H21NO3S
C20H21NO3S
Chemical Communications (2006) 44
a=7.7525(8)Å b=12.0713(13)Å c=9.9335(10)Å
α=90.00° β=97.9140(10)° γ=90.00°
C22H19NOS
C22H19NOS
Chemical Communications (2006) 44
a=9.857(3)Å b=11.082(3)Å c=17.126(5)Å
α=90.00° β=90.00° γ=90.00°
C23H21NOS
C23H21NOS
Chemical Communications (2006) 44
a=9.7025(7)Å b=9.9727(7)Å c=20.1303(15)Å
α=90.00° β=90.00° γ=90.00°
C22H18ClNOS
C22H18ClNOS
Chemical Communications (2006) 44
a=9.6375(5)Å b=10.0167(5)Å c=20.0523(10)Å
α=90.00° β=90.00° γ=90.00°
C24H21NO2S
C24H21NO2S
Chemical communications (Cambridge, England) (2008) 18 2132-2133
a=8.7396(9)Å b=12.0093(13)Å c=19.410(2)Å
α=90.00° β=90.00° γ=90.00°
C18H12O4
C18H12O4
Chemical communications (Cambridge, England) (2009) 34, 17 2379-2380
a=14.8002(10)Å b=8.2800(6)Å c=22.2830(19)Å
α=90.00° β=103.7710(10)° γ=90.00°
C18H12O4
C18H12O4
Chemical communications (Cambridge, England) (2009) 34, 17 2379-2380
a=10.5496(13)Å b=8.5832(10)Å c=14.7098(18)Å
α=90.00° β=98.247(2)° γ=90.00°
C30H28N3O7
C30H28N3O7
RSC Advances (2014)
a=10.4426(6)Å b=12.0149(7)Å c=21.1390(13)Å
α=90.00° β=90.00° γ=90.00°
C45H42Cl3F6Ir2O3P5
C45H42Cl3F6Ir2O3P5
Dalton transactions (Cambridge, England : 2003) (2016) 45, 11 4747-4761
a=15.512(5)Å b=16.476(5)Å c=19.316(6)Å
α=90.0000° β=96.487(4)° γ=90.0000°
C78.50H79Cl3F12Ir2N4P6
C78.50H79Cl3F12Ir2N4P6
Dalton transactions (Cambridge, England : 2003) (2016) 45, 11 4747-4761
a=12.196(3)Å b=17.953(5)Å c=19.765(5)Å
α=99.843(2)° β=96.204(3)° γ=100.923(3)°
C81H84F12Ir2N4P6
C81H84F12Ir2N4P6
Dalton transactions (Cambridge, England : 2003) (2016) 45, 11 4747-4761
a=12.1032(15)Å b=20.671(3)Å c=34.721(4)Å
α=90.0000° β=95.920(2)° γ=90.0000°
C76H79F12Ir2N3P6
C76H79F12Ir2N3P6
Dalton transactions (Cambridge, England : 2003) (2016) 45, 11 4747-4761
a=12.672(2)Å b=16.834(3)Å c=20.346(4)Å
α=75.827(10)° β=74.185(10)° γ=75.401(11)°
C46H42Cl3F6Ir2O4P5
C46H42Cl3F6Ir2O4P5
Dalton transactions (Cambridge, England : 2003) (2016) 45, 11 4747-4761
a=12.621(3)Å b=14.450(3)Å c=14.580(3)Å
α=67.321(8)° β=85.710(8)° γ=88.282(9)°
C79.5H85ClF12Ir2N4O2P6
C79.5H85ClF12Ir2N4O2P6
Dalton transactions (Cambridge, England : 2003) (2016) 45, 11 4747-4761
a=13.7832(17)Å b=14.612(2)Å c=21.817(3)Å
α=81.004(6)° β=74.071(5)° γ=81.207(6)°
[2-Benzylbis(salicylideneiminato)-N,N',O,O']copper(II)
C21H16Cu1N2O2
Acta Crystallographica Section C (1998) 54, 2 191-193
a=16.546(3)Å b=8.970(2)Å c=11.507(2)Å
α=90.00000° β=98.90(2)° γ=90.00000°
C58H50Cl6N2O6
C58H50Cl6N2O6
The Journal of organic chemistry (2018) 83, 2 624-631
a=12.6869(3)Å b=37.5546(12)Å c=11.2665(3)Å
α=90° β=104.367(2)° γ=90°
C16H22BNO3
C16H22BNO3
The Journal of organic chemistry (2019) 84, 19 12532-12541
a=14.8806(19)Å b=10.6387(14)Å c=10.1915(13)Å
α=90° β=97.091(2)° γ=90°
C15H20BNO3
C15H20BNO3
The Journal of organic chemistry (2019) 84, 19 12532-12541
a=10.5088(12)Å b=10.1424(12)Å c=27.846(3)Å
α=90° β=90° γ=90°
C19H22BNO3
C19H22BNO3
The Journal of organic chemistry (2019) 84, 19 12532-12541
a=11.756(4)Å b=17.147(5)Å c=9.519(3)Å
α=90° β=113.778(4)° γ=90°
C18H14N2O2
C18H14N2O2
The Journal of organic chemistry (2019) 84, 19 12532-12541
a=9.0692(9)Å b=9.9319(8)Å c=15.9479(14)Å
α=90.0000° β=90.0000° γ=90.0000°
C23H21N3O3
C23H21N3O3
The Journal of organic chemistry (2019) 84, 11 7362-7371
a=20.7396(4)Å b=8.9839(2)Å c=21.9017(5)Å
α=90° β=90° γ=90°
C32H24O2
C32H24O2
The Journal of organic chemistry (2018) 83, 4 2256-2262
a=10.9306(18)Å b=10.9660(18)Å c=10.9747(18)Å
α=86.834(2)° β=84.597(2)° γ=61.446(2)°
C30H20O2
C30H20O2
The Journal of organic chemistry (2018) 83, 4 2256-2262
a=10.3936(12)Å b=13.0178(16)Å c=16.0441(19)Å
α=100.373(2)° β=92.080(2)° γ=92.163(2)°
C16H12O
C16H12O
The Journal of organic chemistry (2018) 83, 4 2256-2262
a=10.4878(12)Å b=10.7169(12)Å c=10.7804(12)Å
α=90° β=101.988(2)° γ=90°
C32H18F6O2
C32H18F6O2
The Journal of organic chemistry (2018) 83, 4 2256-2262
a=9.0161(9)Å b=9.3663(10)Å c=16.0999(16)Å
α=77.8570(10)° β=85.2310(10)° γ=69.9910(10)°
C32H24O4
C32H24O4
The Journal of organic chemistry (2018) 83, 4 2256-2262
a=9.019(2)Å b=24.900(5)Å c=10.765(2)Å
α=90° β=98.326(3)° γ=90°
C30H18F2O2
C30H18F2O2
The Journal of organic chemistry (2018) 83, 4 2256-2262
a=11.1685(7)Å b=10.7853(7)Å c=18.9822(11)Å
α=90° β=106.1190(10)° γ=90°
C30H20O2
C30H20O2
The Journal of organic chemistry (2018) 83, 4 2256-2262
a=9.9579(11)Å b=17.3275(19)Å c=12.0829(13)Å
α=90° β=96.297(2)° γ=90°
C16H12O2
C16H12O2
The Journal of organic chemistry (2018) 83, 4 2256-2262
a=41.029(4)Å b=9.2510(9)Å c=31.065(3)Å
α=90° β=126.3240(10)° γ=90°
C30H18Cl2O2
C30H18Cl2O2
The Journal of organic chemistry (2018) 83, 4 2256-2262
a=10.6655(18)Å b=15.265(3)Å c=15.421(3)Å
α=71.401(2)° β=76.345(2)° γ=82.394(2)°
C30H20O2
C30H20O2
The Journal of organic chemistry (2018) 83, 4 2256-2262
a=9.9961(9)Å b=10.5492(9)Å c=10.7931(9)Å
α=89.0690(10)° β=65.6050(10)° γ=88.5110(10)°
C15H9FO
C15H9FO
The Journal of organic chemistry (2018) 83, 4 2256-2262
a=3.8335(2)Å b=10.3188(4)Å c=26.6901(11)Å
α=90° β=93.597(2)° γ=90°
C30H18F2O2
C30H18F2O2
The Journal of organic chemistry (2018) 83, 4 2256-2262
a=15.535(3)Å b=7.9072(14)Å c=17.800(3)Å
α=90° β=95.106(3)° γ=90°